Funct. Mater. 2018; 25 (3): 608-612.
Growing and X-ray diffraction pattern of single-crystal double phosphate Li2Mn(PO3)4
1Department of Inorganic Chemistry, T.Shevchenko National University of Kyiv, 64/13 Volodymyrska St., 01601 Kyiv, Ukraine
2National University of Life and Environmental Sciences of Ukraine, 17 Heroyiv Oborony St., 03041 Kyiv, Ukraine
Optimum conditions for the growing of single crystals of Li2Mn(PO3)4 compound have been selected. Complete X-ray diffraction analysis has been performed to study synthesized phosphate Li2Mn(PO3)4. According to its structure, the double phosphate belongs to the orthorhombic crystal system, space group Pnma; lattice parameters are the following: a = 9.268(1), b = 9.421(1), c = 10.088(1), V = 880.93, Z = 4, ρcalc. = 2.901 g/cm3. Structural features of the synthesized phosphate have been determined. The compound has been studied using DTA and IR spectroscopy techniques along with the complete elemental analysis.
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