Funct. Mater. 2023; 30 (2): 178-186.
Investigation of the effect of processing parameters on the spectroscopic properties of ZnSe NCs for hot-pressed ceramics of the Cleartran and Multispectral classes
1Prydniprovska State Academy of Civil Engineering and Architecture, 24a Chernyshevsky Str., 49000 Dnipro, Ukraine
2Kharkiv National Automobile and Highway University, 25 Yaroslava Mudrogo Str., 61002 Kharkiv, Ukraine
3Oles Honchar Dnipro National University, 72 Gagarin Ave., 49010 Dnipro, Ukraine
ZnSe nanocrystals were synthesized by the combustion synthesis method (self-propagating high temperature synthesis) with different initial current pulses. Annealing was carried out in the temperature range T = 200÷800°C with a step of T = 100°C at atmospheric pressure, in air or in nitrogen. The results of electron micrographs, EPR, XRD analysis and photoluminescence depending on the annealing temperature in air or nitrogen are presented. The dependences of the resonance value of the EPR magnetic field of Mn2+ ions, the hyperfine structure constant A of the EPR spectrum of Mn2+ ions, the location of the maximum and the half-width of the integral photoluminescence spectrum on the annealing temperature in air or in nitrogen were obtained. After annealing the nanocrystal size increases by ~ 20 %, the fraction of the cubic phase and the lattice parameter of nanocrystals increase, and both the number of dislocations and microstresses decrease compared to the initial charge. For the synthesis of ZnSe nanocrystals with a more perfect structure, it is recommended to use a current pulse of ~ 40 A followed by annealing at T = 800°C in nitrogen. The obtained results make it possible to use the ZnSe nanocrystals synthesized by the combustion method for various optoelectronic devices or for producing hot-pressed ceramics of the Cleartran or Multispectral classes.
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